HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylcyanamide → HCID 178466076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylcyanamide | HCID 15112 | — |
| Reactant | 4'-Acetyl-2-aminobiphenyl hydrochloride | HCID 19089305 | — |
| Solvent | M-Cresol | HCID 342 | — |
| Product | HCID 178466076 | HCID 178466076 | — |
Reaction Steps
Reaction of dry 4'-acetyl-2-aminobiphenyl hydrochloride (2.6 g) with N,N-dimethylcyanamide (2.5 ml) in m-cresol (7 ml) at 80° C. for 5 hours gave N-(4'-acetyl-2-biphenylyl)-N',N'-dimethylguanidine (2.3 g) as a colourless solid (m.p. 174°-175° C.) which was recrystallised from a mixture of acetone and hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-c9fa1c6364584361998827a21eb5086a |
| Source note | uspto-grants-1994_04 |