HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Cresol → HCID 178484371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | Dimethylcyanamide | HCID 15112 | — |
| Reactant | 3'-fluoro-[1,1'-biphenyl]-2-amine hydrochloride | HCID 2758972 | — |
| Product | HCID 178484371 | HCID 178484371 | — |
Reaction Steps
A mixture of 2-amino-3'-fluorobiphenyl hydrochloride (3.6 g), N,N-dimethylcyanamide (1.7 g) and m-cresol (25 ml) was heated at 90°-95° C. for 8 hours to give N-(3'-fluoro-2-biphenylyl)-N',N'-dimethyl guanidine (m.p. 109°-110° C.) as a colourless solid which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-7efff0c8be2f44cfb08ed6105672d576 |
| Source note | uspto-grants-1994_04 |