Sodium Hydroxide → HCID 19089314, compound

HRID 1464072Notes

Reaction equation

HRID 1464072 reaction equation
C([NH:9][C:10]([NH:12][C:13]1[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=1[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[S:11])(=O)C1C=CC=CC=1.[OH-].[Na+]>C(O)C>[CH3:19][C:18]1[C:13]([NH:12][C:10]([NH2:9])=[S:11])=[C:14]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:15]=[CH:16][CH:17]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 19089190HCID 19089190, compound

Product 1

HCID 19089314HCID 19089314, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of N-benzoyl-N'-(3-methyl-2-biphenylyl)-thiourea (16.2 g), sodium hydroxide (2 g) and ethanol was heated under reflux for two hours to give N-(3-methyl-2-biphenylyl)thiourea as a foamy solid.

Workup

  1. temperaturewas heated
  2. temperatureunder reflux for two hours

Sources & evidence

ORD record
ord-30d8c7da2fd74eeab0a089b3051700bc
Source dataset
uspto-grants-1994_04
Patent number
US05302720

Reaction notes

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