Potassium Hydroxide → HCID 19089247, compound

HRID 1464073Notes

Reaction equation

HRID 1464073 reaction equation
[CH3:1][C:2]1[C:3]([NH:14][C:15]([NH2:17])=S)=[C:4]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1.O.O.O.C([O-])(=O)C.[Pb+2].C([O-])(=O)C.[OH-].[K+]>O>[CH3:1][C:2]1[C:3]([NH:14][C:15]#[N:17])=[C:4]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 14797Potassium HydroxideHCID 22456Lead diacetate trihydrateHCID 19089314HCID 19089314, compound

Product 1

HCID 19089247HCID 19089247, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A mixture of N-(3-methyl-2-biphenylyl)thiourea (11.3 g), lead acetate trihydrate (17.7 g), potassium hydroxide (26.1 g) and water (50 ml) was heated at 90°-95° C. for 30 minutes to give 3-methyl-2-biphenylylcyanamide as a yellow oil.

Workup

  1. temperaturewas heated at 90°-95° C. for 30 minutes

Sources & evidence

ORD record
ord-9175f3a8a0c44cdbb7c2ee6ec0ec4074
Source dataset
uspto-grants-1994_04
Patent number
US05302720

Reaction notes

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