Sodium Hydroxide → HCID 19089277, compound

HRID 1464093Notes

Reaction equation

HRID 1464093 reaction equation
C([NH:9][C:10]([NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[C:19]1[CH:24]=[CH:23][CH:22]=[C:21]([S:25]([CH3:28])(=[O:27])=[O:26])[CH:20]=1)=[S:11])(=O)C1C=CC=CC=1.[OH-].[Na+]>C(O)C>[CH3:28][S:25]([C:21]1[CH:20]=[C:19]([C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=2[NH:12][C:10]([NH2:9])=[S:11])[CH:24]=[CH:23][CH:22]=1)(=[O:27])=[O:26]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 19089216HCID 19089216, compound

Product 1

HCID 19089277HCID 19089277, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of N-benzoyl-N'-(3'-methanesulphonyl-2-biphenylyl)thiourea (8.2 g), sodium hydroxide (0.9 g) and ethanol (20 ml) was heated under reflux for 1.5 hours to give N-(3'-methanesulphonyl-2-biphenylyl)thiourea as a foamy solid.

Workup

  1. temperaturewas heated
  2. temperatureunder reflux for 1.5 hours

Sources & evidence

ORD record
ord-c8b9cebdb2dd4cb6bebfe39de5d52a9f
Source dataset
uspto-grants-1994_04
Patent number
US05302720

Reaction notes

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