Dimethylamine → HCID 178484372, compound

HRID 1464095Notes

Reaction equation

HRID 1464095 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=2[NH:17][C:18]#[N:19])[CH:8]=[CH:9][CH:10]=1)(=[O:4])=[O:3].[CH3:20][NH:21][CH3:22]>>[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=2[NH:17][C:18]([N:21]([CH3:22])[CH3:20])=[NH:19])[CH:8]=[CH:9][CH:10]=1)(=[O:3])=[O:4]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 19089255HCID 19089255, compound

Product 1

HCID 178484372HCID 178484372, compound

Procedure

A mixture of N-(3'-methanesulphonyl-2-biphenylyl)-cyanamide (2.7 g) and 33% ethanolic dimethylamine solution (25 ml) was heated under reflux for 3 hours to give N-(3'-methanesulphonyl-2-biphenylyl)-N',N'-dimethylguanidine (m.p. 113°-114° C.) which was recrystallised from ethylacetate.

Workup

  1. temperaturewas heated
  2. temperatureunder reflux for 3 hours

Sources & evidence

ORD record
ord-93fd0467d2334445afdb01294d8fe223
Source dataset
uspto-grants-1994_04
Patent number
US05302720

Reaction notes

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