HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → 4'-METHOXY-2-NITROBIPHENYL
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Hydroxy-2'-nitrobiphenyl | HCID 15541112 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4'-METHOXY-2-NITROBIPHENYL | HCID 11264685 | — |
Reaction Steps
A mixture of 4'-hydroxy-2-nitrobiphenyl (10.4 g), dimethyl sulphate (9.15 g) in acetone (350 ml) and anhydrous potassium carbonate (22 g) was heated at reflux for 10 hours to get an oil which was purified by column chromatography on silica gel (150 g, 100-200 mesh) eluted with hexane to give 4'-methoxy-2-nitrobiphenyl (m.p. 55°-56° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-d870a40bf2654128b0d37d3d73e8ebe2 |
| Source note | uspto-grants-1994_04 |