HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → N-[[(3,4-dichlorophenyl)amino]carbonyl]-2-thiophenesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 2-Thiophenesulfonamide | HCID 72881 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | N-[[(3,4-dichlorophenyl)amino]carbonyl]-2-thiophenesulfonamide | HCID 19089331 | 39% |
Reaktionsschritte
2-Thiophenesulfonamide (1.55 g, 9.5 mmole) was combined with 3,4-dichlorophenyl isocyanate (1.79 g, 9.5 mmole), 1N NaOH (9.5 ml) and acetone (25 ml) followed by 1N HCl (9.5 ml) using the method of Example 4B to give the named product (1.3 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05302724 |
| Quelldatensatz | uspto-grants-1994_04 |
| ORD ID | ord-2290d93fc6d44ee9b84ed19eacd6d4ea |
| Quellennotiz | uspto-grants-1994_04 |