Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | BIS(TRIMETHYLSILYLMETHYL)DICHLOROSILANE | HCID 11747735 | — |
| Product | HCID 11747608 | HCID 11747608 | 74% |
Reaction Steps
13.7 g(50 mmoles) of 2,2,6,6-tetramethyl-4,4-dichloro-2,4,6-trisilaheptane were placed in the flask of the same set as Example 1, and then 1.8 g(60 mmoles) of dry methanol were added. The mixture was heated at 70° C. for 2 hrs. The amount of the product was 9.92 g and the yield 74%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05302734 |
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| Source dataset | uspto-grants-1994_04 |
|---|
| ORD ID | ord-b6efa47268994222961eb742258b7bf6 |
|---|
| Source note | uspto-grants-1994_04 |
|---|
