HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Tyrosine ethyl ester → HCID 178472556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Tyrosine ethyl ester | HCID 70364 | — |
| Reactant | HCID 178472567 | HCID 178472567 | — |
| Product | HCID 178472556 | HCID 178472556 | 75% |
Reaction Steps
In a batch procedure (300 l), Mal-Tyr-OEt (0.25M) and Arg-OEt (0.25M) are reacted with α-chymotrypsin (0.025 mg/ml) at pH 9.5 and 25° C. After 2 hours, filtration of the precipitate and washing with water result in 26.0 kg of Mal-Tyr-Arg-OEt (75% of theoretical yield) with an HPLC purity greater than 97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304470 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-ee7ab821a415472382e7352f6b8b4381 |
| Source note | uspto-grants-1994_04 |