HCID 11593563, compound → HCID 15713969, compound

HRID 1464258Notes

Reaction equation

HRID 1464258 reaction equation
C1(CC(O)=O)C2C(=CC=CC=2)C=NN=1.C([O:17][C:18](=[O:46])[CH2:19][C:20]1[C:29]2[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=2)[C:23](=[O:30])[N:22]([CH2:31][C:32]([NH:34][C:35]2[CH:40]=[C:39]([C:41]([F:44])([F:43])[F:42])[CH:38]=[CH:37][C:36]=2[Br:45])=[S:33])[N:21]=1)C>>[Br:45][C:36]1[CH:37]=[CH:38][C:39]([C:41]([F:44])([F:42])[F:43])=[CH:40][C:35]=1[NH:34][C:32](=[S:33])[CH2:31][N:22]1[C:23](=[O:30])[C:24]2[C:29](=[CH:28][CH:27]=[CH:26][CH:25]=2)[C:20]([CH2:19][C:18]([OH:46])=[O:17])=[N:21]1

Participants

3

Reactant 2

HCID 11593563HCID 11593563, compoundHCID 15713968HCID 15713968, compound

Product 1

HCID 15713969HCID 15713969, compound

Procedure

This compound was prepared according to Example 3, starting with 1-phthalazine acetic acid, 3-[2-[N-[2-bromo-5-(trifluoromethyl) phenyl]amino]-2-thioxoethyl]-3,4-dihydro-4-oxo-, ethyl ester (0.15 g) [the final product of Example 5]. The title compound melted at 176°-177° C. (yield, 0.12 g) .

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-d48f1f1fd65c404082e38b32215087f3
Source dataset
uspto-grants-1994_04
Patent number
US05304557

Reaction notes

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