Sodium Hydroxide → HCID 19087792, compound

HRID 1464385Notes

Reaction equation

HRID 1464385 reaction equation
[F:1][C:2]([F:29])([F:28])[S:3][C:4]1[CH:5]=[C:6]([CH2:22][C:23]([O:25]CC)=[O:24])[CH:7]=[CH:8][C:9]=1[O:10][CH2:11][C:12]1[CH:21]=[CH:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[N:13]=1.[OH-].[Na+]>O1CCOCC1.O>[F:28][C:2]([F:1])([F:29])[S:3][C:4]1[CH:5]=[C:6]([CH2:22][C:23]([OH:25])=[O:24])[CH:7]=[CH:8][C:9]=1[O:10][CH2:11][C:12]1[CH:21]=[CH:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[N:13]=1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 19087777HCID 19087777, compound

Product 1

HCID 19087792HCID 19087792, compound

Reagents, catalysts & solvents 1

HCID 218864351,4-Dioxane--water (1/1)Solvent

Procedure

In analogy to the procedure of Example XV, the title compound is prepared from 2.1 g (5 mmol) of the compound from Example XXV and 0.4 g (0.01 mol) of sodium hydroxide in dioxane/water.

Sources & evidence

ORD record
ord-eeb55960a3c64b2f8fbdf10a74414159
Source dataset
uspto-grants-1994_04
Patent number
US05304563

Reaction notes

Loading…