HCID 19087770, compound → HCID 19087783, compound

HRID 1464396Notes

Reaction equation

HRID 1464396 reaction equation
[CH2:1]([C:4]1[CH:5]=[C:6]([CH2:22][C:23]([O:25][CH3:26])=[O:24])[CH:7]=[CH:8][C:9]=1[O:10][CH2:11][C:12]1[CH:21]=[CH:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[N:13]=1)[CH:2]=[CH2:3].[H][H]>[Pd]>[CH2:1]([C:4]1[CH:5]=[C:6]([CH2:22][C:23]([O:25][CH3:26])=[O:24])[CH:7]=[CH:8][C:9]=1[O:10][CH2:11][C:12]1[CH:21]=[CH:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[N:13]=1)[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 19087770HCID 19087770, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 19087783HCID 19087783, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

In analogy to the procedure of Example XXXIV, the title compound is prepared from 7.5 g (0.0225 mol) of the compound from Example XXXVII and 0.8 g of Pd/C (5%) using hydrogen.

Sources & evidence

ORD record
ord-81363ff1205a41768579e1e54500e092
Source dataset
uspto-grants-1994_04
Patent number
US05304563

Reaction notes

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