HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoamyl Nitrite → 2-Methyl-4-nitrosoresorcinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Reactant | 2-Methylresorcinol | HCID 11843 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Methyl-4-nitrosoresorcinol | HCID 100616 | — |
Reaction Steps
19.8 g. 2-Methylresorcinol and 13.4 g. potassium hydroxide are dissolved in 120 ml. ethanol and cooled to 5° C. 24 ml. Isopentyl nitrite are added dropwise thereto, the reaction mixture is stirred for 3 hours and the precipitate is filtered off with suction. The yellow solid material is stirred into 200 ml. 5N sulphuric acid, the bright yellow product thereby precipitating out. Yield 22 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304645 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-63c2a46ced484bca92e3fbc8bb0f2b1c |
| Source note | uspto-grants-1994_04 |