HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 5,6-Dihydro-4H-cyclopenta[b]thiophene-2-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4H,5H,6H-cyclopenta(b)thiophene-2-carboxylic acid | HCID 770980 | — |
| Product | 5,6-Dihydro-4H-cyclopenta[b]thiophene-2-carbonyl chloride | HCID 19088019 | — |
Reaction Steps
1.0 g of 5,6-dihydro-4H-cyclopenta[b]thiophene-2-carboxylic acid was reacted with 4 ml of thionyl chloride for 3.5 hours under reflux. Then, excess thionyl chloride was distilled off under reduced pressure to obtain 5,6-dihydro-4H-cyclopenta[b]thiophene-2-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304657 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-c9cecca69b4e49e7a0992b094561e098 |
| Source note | uspto-grants-1994_04 |