HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 2-Nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde dimethylacetal | HCID 19086863 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde | HCID 19086846 | — |
Reaction Steps
0.3 Gram of 2-nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde dimethylacetal, 5 ml of formalin, 1 ml of ethanol and 2 drops of concentrated hydrochloric acid were refluxed by heating. After the reaction was completed, the solvent was removed by evaporation to obtain the residue, then water was added to the residue. The crystals formed were collected by filtration to yield 0.22 g of 2-nitro-5-(4-acetylamino-1-piperidyl)benzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306719 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-24500cb7809f4f38bdc83cb7fb68bc53 |
| Source note | uspto-grants-1994_04 |