HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 67655879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | HCID 10085154 | HCID 10085154 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 67655879 | HCID 67655879 | — |
Reaction Steps
A solution of 4'-methoxy-2-[(trifluoromethyl)sulfonyl]acetophenone (6.0 g, 0.021 mol) in toluene is treated with aminoacetaldehyde diethyl acetal (2.8 g, 0.021 mol), heated at reflux overnight with removal of water, and concentrated in vacuo to obtain the title product as an oil. This oil is used in Example 4 without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306827 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-db8fc4ae63ae415095cec7773249b8b8 |
| Source note | uspto-grants-1994_04 |