3-Bromoaniline → HCID 19917176, compound

HRID 1464758Notes

Reaction equation

HRID 1464758 reaction equation
BrC1C=[C:4]([SH:8])[CH:5]=[CH:6][CH:7]=1.BrC1C=C(C=CC=1)N.Br[C:18]1[CH:19]=[C:20]([CH:28]=[CH:29][CH:30]=1)[O:21][CH2:22][C:23]([O:25]CC)=[O:24].S1C=CC(C2C=C(CC(O)=S)C=CC=2)=C1.S1C=CC(C2C=C(NCC(O)=O)C=CC=2)=C1>>[S:8]1[CH:7]=[CH:6][C:5]([C:18]2[CH:19]=[C:20]([CH:28]=[CH:29][CH:30]=2)[O:21][CH2:22][C:23]([OH:25])=[O:24])=[CH:4]1

Participants

6

Reactant 5

HCID 115623-BromoanilineHCID 80597m-BromobenzenethiolHCID 5197439Ethyl 2-(3-bromophenoxy)acetateHCID 19917027HCID 19917027, compoundHCID 178526158HCID 178526158, compound

Product 1

HCID 19917176HCID 19917176, compound

Procedure

When the same reactions as in Referential Example 12 are carried out using 3-bromothiophenol or 3-bromoaniline instead of the starting 3-bromophenol, 3-(3-thienyl)phenylthioacetic acid and 3-(3-thienyl)phenylaminoacetic acid are obtained.

Workup

  1. customare obtained

Sources & evidence

ORD record
ord-3262002137bd4be7b36dd6451982ef1a
Source dataset
uspto-grants-1994_04
Patent number
US05306728

Reaction notes

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