HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[3-(3-Thienyl)phenyl]-1-propanol → 3-[3-(3-Thienyl)phenyl]propanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[3-(3-Thienyl)phenyl]-1-propanol | HCID 19917076 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-[3-(3-Thienyl)phenyl]propanal | HCID 19917149 | 77.4% |
Reaction Steps
150 mg of the resulting alcohol compound was dissolved in 5 ml of chloroform, and 222 mg of pyridinium chlorochromate was added. The mixture was stirred overnight at room temperature, and then the s precipitate was removed by filtration. The filtrate was Worked up in a customary manner, and the product was purified by silica gel column chromatography [hexane/ethyl acetate=5/1] to give 115 mg Of the captioned compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306728 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-814ca39d43374f18801468b9cb618ea7 |
| Source note | uspto-grants-1994_04 |