Tetrahydrofuran → HCID 19917135, compound

Participants

Reaction Steps

0.48 g of the resulting alcohol compound was dissolved in 5 ml of tetarahydrofuran, and under a nitrogen atmosphere, a tetrahydrofuran solution (5 ml) of 78 mg of lithium aluminum hydride was added. The mixture was stirred under ice cooling for 2 hours, and then at room temperature for 1 hour. Ethyl acetate and water were added, and the organic layer separated was worked up in a customary manner. The product was purified by silica gel column chromatography [hexane / ethyl acetate=4/1] to give 0.28 g of the captioned compound as a colorless oil.

Provenance & Evidence