HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53668277, compound → HCID 54118311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53668277 | HCID 53668277 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54118311 | HCID 54118311 | — |
Reaction Steps
A solution of (S)-4-benzyl-3-[(1S)-2-(4-benzyloxyphenyl)-1-phenoxyethyl]-2-oxazolidinone (1.8 g) in ethyl acetate (50 ml) containing 10% palladium on carbon (1.8 g) was hydrogenated at 40 psi overnight. The catalyst was filtered, the solution concentrated and the product purified by flash chromatography (hexanes/ethyl acetate, 3:2) as an oil (0.81 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306726 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-e4a9ef63e2744d3f88ee6d91a604f688 |
| Source note | uspto-grants-1994_04 |