HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 565655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,8-Octanediamine | HCID 24250 | — |
| Reactant | 2-Furancarbonyl chloride | HCID 68242 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Product | HCID 565655 | HCID 565655 | — |
Reaction Steps
The general procedure was carried out using 1,8-octanediamine (10.0 g, 69.3 mmol), triethylamine (14.2 g, 141 mmol), DMAP (0.17 g, 1.35 mmol) and furoyl chloride (19.0 g, 146 mmol). The resulting compound was purified by column chromatography (98:2 DCM:EtOAc), and the product obtained as a white solid (21.5 g/92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999444B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-1c387d9c54e646a1a00497edfc025747 |
| Source note | uspto-grants-2015_04 |