3,4,5-Trimethoxyaniline → HCID 67362316, compound

HRID 1464993Notes

Reaction equation

HRID 1464993 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:20])[NH:9][C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([C:16]([F:19])([F:18])[F:17])[CH:11]=2)=[CH:4][C:3]=1[NH:21][C:22]([C:24]1[C:28]2[N:29]=[CH:30][N:31]=[C:32](S(C)=O)[C:27]=2[S:26][CH:25]=1)=[O:23].[CH3:36][O:37][C:38]1[CH:39]=[C:40]([CH:42]=[C:43]([O:47][CH3:48])[C:44]=1[O:45][CH3:46])[NH2:41]>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:20])[NH:9][C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([C:16]([F:19])([F:17])[F:18])[CH:11]=2)=[CH:4][C:3]=1[NH:21][C:22]([C:24]1[C:28]2[N:29]=[CH:30][N:31]=[C:32]([NH:41][C:40]3[CH:42]=[C:43]([O:47][CH3:48])[C:44]([O:45][CH3:46])=[C:38]([O:37][CH3:36])[CH:39]=3)[C:27]=2[S:26][CH:25]=1)=[O:23]

Participants

3

Reactant 2

HCID 322853,4,5-TrimethoxyanilineHCID 68263099HCID 68263099, compound

Product 1

HCID 67362316HCID 67362316, compound

Procedure

The procedure of Step 3 of Example 13 was repeated except for using the compound obtained in Step 2 of Example 13 and 3,4,5-trimethoxyaniline to obtain the title compound (see Table 1).

Sources & evidence

ORD record
ord-943592ebdcd648bc9736b89314ec1559
Source dataset
uspto-grants-2015_04
Patent number
US08999973B2

Reaction notes

Loading…