Hydrazine → HCID 67518029, compound

Participants

Reaction Conditions

Reaction Steps

The mixture of methyl 3-(2-methylpyridin-4-yl)-1-trityl-1H-indazole-5-carboxylate (50 mg, 0.1 mmol) and hydrazine (6.3 mg, 0.2 mmol) in DMF (0.23 mL) was heated at 100° C. under microwave condition for 45 min. The reaction mixture was quenched with water, and extracted with EtOAc. The combined organic layer was dried and concentrated to give 52 mg of crude product. The crude was brought to next step without further purification.

Provenance & Evidence