HCID 178450842, compound → HCID 11847514, compound

HRID 1465923Notes

Reaction equation

HRID 1465923 reaction equation
C(O[C:6]([C:8]1[C:9]([OH:26])=[C:10]2[CH:17]=[C:16]([C:18]3[CH:23]=[CH:22][C:21]([O:24][CH3:25])=[CH:20][CH:19]=3)[S:15][C:11]2=[C:12](O)[N:13]=1)=[O:7])CCC.C([O:31][C:32]([C:34]1[N:39]=C(O)C2C=C(C3C=CC(OC)=CC=3)SC=2C=1O)=[O:33])CCC>>[OH:26][C:9]1[C:8]([C:6]([NH:39][CH2:34][C:32]([OH:33])=[O:31])=[O:7])=[N:13][CH:12]=[C:11]2[S:15][C:16]([C:18]3[CH:19]=[CH:20][C:21]([O:24][CH3:25])=[CH:22][CH:23]=3)=[CH:17][C:10]=12

Participants

3

Reactant 2

HCID 178450842HCID 178450842, compoundHCID 178450864HCID 178450864, compound

Product 1

HCID 11847514HCID 11847514, compound

Procedure

The title compound was prepared from a mixture of 4,7-dihydroxy-2-(4-methoxy-phenyl)-thieno[2,3-c]pyridine-5-carboxylic acid butyl ester and 4,7-dihydroxy-2-(4-methoxy-phenyl)-thieno[3,2-c]pyridine-6-carboxylic acid butyl ester, example 3-b, under conditions analogous to experimental example 1-f. MS: (+) m/z 390.24, 392.19 (M+1, 35Cl/37Cl).

Sources & evidence

ORD record
ord-2c61c636a8e34ebc907754e231ebed94
Source dataset
uspto-grants-2015_04
Patent number
US09000006B2

Reaction notes

Loading…