HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 77230699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 69087457 | HCID 69087457 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 77230699 | HCID 77230699 | — |
Reaction Steps
A solution of 4-Allyl-2-chlorobenzonitrile (265 mg, 1.5 mmol) in DCM (2 mL) and methanol (2 mL) was cooled to −78° C. Then O3 was bubbled into for 10 minutes. Then dimethylsulfide (1 mL) was added and the mixture was stirred at RT for 5 hours. The mixture was concentrated in vacuo to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999990B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-13bf2f95a92240fcb20bbaf824afae85 |
| Source note | uspto-grants-2015_04 |