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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1466031Generated: November 2, 2026

Methanol → HCID 77230699, compound

https://huagongshe.com/reaction/1466031

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 69087457HCID 69087457—
SolventDichloromethaneHCID 6344—
ProductHCID 77230699HCID 77230699—

Reaction Steps

A solution of 4-Allyl-2-chlorobenzonitrile (265 mg, 1.5 mmol) in DCM (2 mL) and methanol (2 mL) was cooled to −78° C. Then O3 was bubbled into for 10 minutes. Then dimethylsulfide (1 mL) was added and the mixture was stirred at RT for 5 hours. The mixture was concentrated in vacuo to give the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08999990B2
Source datasetuspto-grants-2015_04
ORD IDord-13bf2f95a92240fcb20bbaf824afae85
Source noteuspto-grants-2015_04