Ethanol → HCID 66765172, compound

Participants

Reaction Steps

[3-(1-Benzyl-6-chloro-2-methyl-1H-indol-3-yloxy)-phenyl]-acetonitrile (0.065 g, 0.168 mmol) was dissolved in EtOH (3 mL) then acetyl chloride (0.240 mL, 3.36 mmol) was added and the reaction was heated to reflux for 3 days. After cooling the reaction was submitted to aqueous workup and silica gel chromatography to afford the title compound.

Provenance & Evidence