2-(Chloromethyl)-3,5-dimethyl-4-methoxypyridine hydrochloride → HCID 66765326, compound

HRID 1466796Notes

Reaction equation

HRID 1466796 reaction equation
[CH3:1][O:2][C:3](=[O:22])[C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([S:10][C:11]2[C:19]3[C:14](=[CH:15][C:16]([Cl:20])=[CH:17][CH:18]=3)[NH:13][C:12]=2[CH3:21])[CH:5]=1.Cl.Cl[CH2:25][C:26]1[C:31]([CH3:32])=[C:30]([O:33][CH3:34])[C:29]([CH3:35])=[CH:28][N:27]=1>>[CH3:1][O:2][C:3](=[O:22])[C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([S:10][C:11]2[C:19]3[C:14](=[CH:15][C:16]([Cl:20])=[CH:17][CH:18]=3)[N:13]([CH2:25][C:26]3[C:31]([CH3:32])=[C:30]([O:33][CH3:34])[C:29]([CH3:35])=[CH:28][N:27]=3)[C:12]=2[CH3:21])[CH:5]=1

Participants

3

Reactant 2

HCID 116942582-(Chloromethyl)-3,5-dimethyl-4-methoxypyridine hydrochlorideHCID 66765016HCID 66765016, compound

Product 1

HCID 66765326HCID 66765326, compound

Procedure

Prepared according to the procedure described in Example 24, Step 1, using the following starting materials: 3-(6-chloro-2-methyl-1H-indol-3-ylsulfanyl)-benzoic acid methyl ester and 2-chloromethyl-4-methoxy-3,5-dimethyl-pyridine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c7ed9fef47fa4913b2e282c8d0c48097
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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