m-Chlorophenylhydrazine hydrochloride → HCID 66765411, compound

HRID 1466831Notes

Reaction equation

HRID 1466831 reaction equation
[CH2:1]([O:3][C:4](=[O:20])[C:5]1[CH:10]=[C:9]([C:11]([F:14])([F:13])[F:12])[CH:8]=[C:7]([S:15][CH2:16][C:17](=O)[CH3:18])[CH:6]=1)[CH3:2].Cl.[Cl:22][C:23]1[CH:24]=[C:25]([NH:29]N)[CH:26]=[CH:27][CH:28]=1>>[CH2:1]([O:3][C:4](=[O:20])[C:5]1[CH:10]=[C:9]([C:11]([F:14])([F:13])[F:12])[CH:8]=[C:7]([S:15][C:16]2[C:26]3[C:25](=[CH:24][C:23]([Cl:22])=[CH:28][CH:27]=3)[NH:29][C:17]=2[CH3:18])[CH:6]=1)[CH3:2]

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 66764760HCID 66764760, compound

Product 1

HCID 66765411HCID 66765411, compound

Procedure

Prepared according to the procedure described in Example 10, Step 2, using the following starting materials: 3-(2-oxo-propylsulfanyl)-5-trifluoromethyl-benzoic acid ethyl ester and 3-chlorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-7af58ec22ad942cf8f72d033203b24a7
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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