m-Chlorophenylhydrazine hydrochloride → HCID 66765306, compound

HRID 1466835Notes

Reaction equation

HRID 1466835 reaction equation
[CH2:1]([O:3][C:4](=[O:19])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([S:14][CH2:15][C:16](=O)[CH3:17])[CH:7]=1)[CH3:2].Cl.[Cl:21][C:22]1[CH:23]=[C:24]([NH:28]N)[CH:25]=[CH:26][CH:27]=1>>[CH2:1]([O:3][C:4](=[O:19])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8]([S:14][C:15]2[C:25]3[C:24](=[CH:23][C:22]([Cl:21])=[CH:27][CH:26]=3)[NH:28][C:16]=2[CH3:17])[CH:7]=1)[CH3:2]

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 66764935HCID 66764935, compound

Product 1

HCID 66765306HCID 66765306, compound

Procedure

Prepared according to the procedure described in Example 10, Step 2, using the following starting materials: [4-methoxy-3-(2-oxo-propylsulfanyl)-phenyl]-acetic acid ethyl ester and 3-chlorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-c60329c3548147d7a63419df81310bbc
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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