m-Chlorophenylhydrazine hydrochloride → 3-(6-Chloro-2-methyl-1H-indol-3-ylsulfanyl)-2-methoxy-benzoic acid ethyl ester

HRID 1466856Notes

Reaction equation

HRID 1466856 reaction equation
[CH2:1]([O:3][C:4](=[O:18])[C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([S:11][CH2:12][C:13](=O)[CH3:14])[C:6]=1[O:16][CH3:17])[CH3:2].Cl.[Cl:20][C:21]1[CH:22]=[C:23]([NH:27]N)[CH:24]=[CH:25][CH:26]=1>>[CH2:1]([O:3][C:4](=[O:18])[C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([S:11][C:12]2[C:24]3[C:23](=[CH:22][C:21]([Cl:20])=[CH:26][CH:25]=3)[NH:27][C:13]=2[CH3:14])[C:6]=1[O:16][CH3:17])[CH3:2]

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 667650372-Methoxy-3-(2-oxo-propylsulfanyl)-benzoic acid ethyl ester

Product 1

HCID 667648883-(6-Chloro-2-methyl-1H-indol-3-ylsulfanyl)-2-methoxy-benzoic acid ethyl ester

Procedure

Prepared according to the procedure described in Example 2, Step 1, using the following starting materials: 2-Methoxy-3-(2-oxo-propylsulfanyl)-benzoic acid ethyl ester and 3-chlorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-8ef9d46d67a3413a9b87c5d71ad7f45d
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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