3-Chloro-6-methylpyridazine → HCID 66764886, compound

HRID 1466866Notes

Reaction equation

HRID 1466866 reaction equation
[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([S:11][C:12]2[C:20]3[C:15](=[CH:16][C:17]([Cl:21])=[CH:18][CH:19]=3)[NH:14][C:13]=2[CH3:22])[CH:6]=1)[CH3:2].Cl[C:25]1[N:26]=[N:27][C:28]([CH3:31])=[CH:29][CH:30]=1>>[CH2:1]([O:3][C:4](=[O:23])[C:5]1[CH:10]=[CH:9][CH:8]=[C:7]([S:11][C:12]2[C:20]3[C:15](=[CH:16][C:17]([Cl:21])=[CH:18][CH:19]=3)[N:14]([C:25]3[N:26]=[N:27][C:28]([CH3:31])=[CH:29][CH:30]=3)[C:13]=2[CH3:22])[CH:6]=1)[CH3:2]

Participants

3

Reactant 2

HCID 2272543-Chloro-6-methylpyridazineHCID 667654983-(6-Chloro-2-methyl-1H-indol-3-ylsulfanyl)-benzoic acid ethyl ester

Product 1

HCID 66764886HCID 66764886, compound

Procedure

Prepared according to the procedure described in Example 55, Step 2 using the following starting materials: 3-(6-chloro-2-methyl-1H-indol-3-ylsulfanyl)-benzoic acid ethyl ester and 3-chloro-6-methyl-pyridazine.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-79c686196d5d4c43a88a221c5906af2b
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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