m-Chlorophenylhydrazine hydrochloride → HCID 66765116, compound

HRID 1466872Notes

Reaction equation

HRID 1466872 reaction equation
[CH2:1]([O:3][C:4]([C:6]1([C:9]2[CH:14]=[CH:13][CH:12]=[C:11]([S:15][CH2:16][C:17](=O)[CH3:18])[CH:10]=2)[CH2:8][CH2:7]1)=[O:5])[CH3:2].Cl.[Cl:21][C:22]1[CH:23]=[C:24]([NH:28]N)[CH:25]=[CH:26][CH:27]=1>>[CH2:1]([O:3][C:4]([C:6]1([C:9]2[CH:14]=[CH:13][CH:12]=[C:11]([S:15][C:16]3[C:25]4[C:24](=[CH:23][C:22]([Cl:21])=[CH:27][CH:26]=4)[NH:28][C:17]=3[CH3:18])[CH:10]=2)[CH2:8][CH2:7]1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 66765113HCID 66765113, compound

Product 1

HCID 66765116HCID 66765116, compound

Procedure

Prepared according to the procedure described in Example 2, Step 1, using the following starting materials: 1-[3-(2-oxo-propylsulfanyl)-phenyl]-cyclopropanecarboxylic acid ethyl ester and 3-chlorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-75c990ae83d34dfbaec426222d0a404a
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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