m-Chlorophenylhydrazine hydrochloride → 3-(3-Bromo-phenylsulfanyl)-6-chloro-2-ethyl-1H-indole

HRID 1466906Notes

Reaction equation

HRID 1466906 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([S:8][CH2:9][C:10](=O)[CH2:11][CH3:12])[CH:5]=[CH:6][CH:7]=1.Cl.[Cl:15][C:16]1[CH:17]=[C:18]([NH:22]N)[CH:19]=[CH:20][CH:21]=1>>[Br:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[C:19]3[C:18](=[CH:17][C:16]([Cl:15])=[CH:21][CH:20]=3)[NH:22][C:10]=2[CH2:11][CH3:12])[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 628042481-((3-Bromophenyl)thio)butan-2-one

Product 1

HCID 667652053-(3-Bromo-phenylsulfanyl)-6-chloro-2-ethyl-1H-indole

Procedure

Prepared according to the procedure described in Example 2, Step 1, using the following starting materials: 1-(3-bromo-phenylsulfanyl)-butan-2-one and 3-chlorophenylhydrazine hydrochloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-a6ea7afee1734f0eb6e4fda7674c1d90
Source dataset
uspto-grants-2015_04
Patent number
US09000025B2

Reaction notes

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