HuagongsheHuagongshe Chemistry Print Report · For research reference only
(R)-(-)-2-Amino-1-propanol → HCID 66746385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (R)-(-)-2-Amino-1-propanol | HCID 80308 | — |
| Reactant | 2-Amino-6-fluorobenzonitrile | HCID 522659 | — |
| Product | HCID 66746385 | HCID 66746385 | — |
Reaction Steps
Prepared as in Example 24d from (R)-2-aminopropan-1-ol and 2-amino-6-fluoro-benzonitrile as brown solid (81%). 1H NMR (400 MHz, DMSO-d6) δ 1.01 (d, J=6.5 Hz, 3H), 3.08 (m, 1H), 3.71 (d, J=6.1 Hz, 2H), 5.95 (s, 2H), 6.15 (d, J=8.3 Hz, 1H), 6.2 (d, J=8.3 Hz, 1H), 7.13 (t, J=8.3 Hz, 1H). MS 192 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09000054B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-cf6596d35e4a45aa9baf5b81d2298056 |
| Source note | uspto-grants-2015_04 |