2-Cyclohexen-1-OL → HCID 66747185, compound

HRID 1467153Notes

Reaction equation

HRID 1467153 reaction equation
[CH:1]1([OH:7])[CH2:6][CH2:5][CH2:4][CH:3]=[CH:2]1.[N+:8]([C:11]1[CH:18]=[CH:17][CH:16]=[C:15]([N+]([O-])=O)[C:12]=1[C:13]#[N:14])([O-:10])=[O:9]>>[CH:1]1([O:7][C:15]2[CH:16]=[CH:17][CH:18]=[C:11]([N+:8]([O-:10])=[O:9])[C:12]=2[C:13]#[N:14])[CH2:6][CH2:5][CH2:4][CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 131982-Cyclohexen-1-OLHCID 520718Dinitrobenzonitrile

Product 1

HCID 66747185HCID 66747185, compound

Procedure

Prepared as in Example 126c from cyclohex-2-enol and 2,6-dinitrobenzonitrile as a brown solid (90%). MS 245 (MH+).

Sources & evidence

ORD record
ord-f8fb5ec779d9430ca66ce144e3a169c9
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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