4-Hydroxycyclohexanecarboxylic acid → HCID 66746578, compound

HRID 1467181Notes

Reaction equation

HRID 1467181 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][CH:5]([C:8]([OH:10])=[O:9])[CH2:4][CH2:3]1.[N+:11]([C:14]1[CH:21]=[CH:20][CH:19]=[C:18]([N+]([O-])=O)[C:15]=1[C:16]#[N:17])([O-:13])=[O:12]>>[C:16]([C:15]1[C:14]([N+:11]([O-:13])=[O:12])=[CH:21][CH:20]=[CH:19][C:18]=1[O:1][CH:2]1[CH2:7][CH2:6][CH:5]([C:8]([OH:10])=[O:9])[CH2:4][CH2:3]1)#[N:17]

Participants

3

Reactant 2

HCID 1511384-Hydroxycyclohexanecarboxylic acidHCID 520718Dinitrobenzonitrile

Product 1

HCID 66746578HCID 66746578, compound

Procedure

Prepared as in Example 47d from 4-hydroxycyclohexanecarboxylic acid and 2,6-dinitrobenzonitrile as a brown solid (50%). MS 291 (MH+).

Sources & evidence

ORD record
ord-6374b94e26d443dabb55bb95b1f89462
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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