Propyl isocyanate → HCID 66745847, compound

HRID 1467232Notes

Reaction equation

HRID 1467232 reaction equation
[Cl-].[C:2]([C:4]1[C:16]([N+:17]([O-])=O)=[CH:15][CH:14]=[CH:13][C:5]=1[O:6][CH2:7][C@@H:8]1[CH2:12][CH2:11][CH2:10][NH2+:9]1)#[N:3].[CH2:20]([N:23]=[C:24]=[O:25])[CH2:21][CH3:22]>>[NH2:17][C:16]1[C:4]([C:2]#[N:3])=[C:5]([CH:13]=[CH:14][CH:15]=1)[O:6][CH2:7][C@@H:8]1[CH2:12][CH2:11][CH2:10][N:9]1[C:24]([NH:23][CH2:20][CH2:21][CH3:22])=[O:25]

Participants

3

Reactant 2

HCID 61033Propyl isocyanateHCID 66747036HCID 66747036, compound

Product 1

HCID 66745847HCID 66745847, compoundYield 100%

Procedure

Prepared as in Example 191a from (S)-2-((2-cyano-3-nitrophenoxy)methyl)pyrrolidinium chloride (Example 191b) and propyl isocyanate in 100% yield as a white solid. MS 303 (MH+).

Sources & evidence

ORD record
ord-ee93878dbe994f72bd92b7afd398653c
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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