Dinitrobenzonitrile → HCID 66747141, compound

HRID 1467245Notes

Reaction equation

HRID 1467245 reaction equation
[OH:1][CH2:2][C:3]([CH3:12])([CH3:11])[C:4]([NH:6][CH2:7][CH2:8][O:9][CH3:10])=[O:5].[N+:13]([C:16]1[CH:23]=[CH:22][CH:21]=[C:20]([N+]([O-])=O)[C:17]=1[C:18]#[N:19])([O-:15])=[O:14]>>[C:18]([C:17]1[C:16]([N+:13]([O-:15])=[O:14])=[CH:23][CH:22]=[CH:21][C:20]=1[O:1][CH2:2][C:3]([CH3:12])([CH3:11])[C:4]([NH:6][CH2:7][CH2:8][O:9][CH3:10])=[O:5])#[N:19]

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 86657476HCID 86657476, compound

Product 1

HCID 66747141HCID 66747141, compoundYield 55%

Procedure

Prepared as in Example 197c from 3-hydroxy-N-(2-methoxyethyl)-2,2-dimethylpropanamide (Example 204d) and 2,6-dinitrobenzonitrile in 55% yield. MS 322 (MH+).

Sources & evidence

ORD record
ord-db0f87831c7646ae94e03c71ad8775b7
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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