Dinitrobenzonitrile → HCID 66747217, compound

HRID 1467247Notes

Reaction equation

HRID 1467247 reaction equation
[OH:1][CH2:2][C:3]([CH3:11])([CH3:10])[CH2:4][NH:5][C:6](=[O:9])[CH2:7][CH3:8].[N+:12]([C:15]1[CH:22]=[CH:21][CH:20]=[C:19]([N+]([O-])=O)[C:16]=1[C:17]#[N:18])([O-:14])=[O:13]>>[C:17]([C:16]1[C:15]([N+:12]([O-:14])=[O:13])=[CH:22][CH:21]=[CH:20][C:19]=1[O:1][CH2:2][C:3]([CH3:10])([CH3:11])[CH2:4][NH:5][C:6](=[O:9])[CH2:7][CH3:8])#[N:18]

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 81646287HCID 81646287, compound

Product 1

HCID 66747217HCID 66747217, compoundYield 68%

Procedure

Prepared as in Example 197c from N-(3-hydroxy-2,2-dimethylpropyl)propionamide (Example 205c) and 2,6-dinitrobenzonitrile in 68% yield. MS 306 (MH+).

Sources & evidence

ORD record
ord-6a89475ed7c04c8da3a5c8a33bb5d3f3
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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