Dinitrobenzonitrile → HCID 66746203, compound

HRID 1467248Notes

Reaction equation

HRID 1467248 reaction equation
[CH2:1]([NH:3][C:4]([NH:6][CH2:7][C:8]([CH3:12])([CH3:11])[CH2:9][OH:10])=[O:5])[CH3:2].[N+:13]([C:16]1[CH:23]=[CH:22][CH:21]=[C:20]([N+]([O-])=O)[C:17]=1[C:18]#[N:19])([O-:15])=[O:14]>>[C:18]([C:17]1[C:16]([N+:13]([O-:15])=[O:14])=[CH:23][CH:22]=[CH:21][C:20]=1[O:10][CH2:9][C:8]([CH3:11])([CH3:12])[CH2:7][NH:6][C:4]([NH:3][CH2:1][CH3:2])=[O:5])#[N:19]

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 22381395HCID 22381395, compound

Product 1

HCID 66746203HCID 66746203, compoundYield 47%

Procedure

Prepared as in Example 197c from 1-ethyl-3-(3-hydroxy-2,2-dimethylpropyl)urea (Example 206d) and 2,6-dinitrobenzonitrile in 47% yield. MS 321 (MH+).

Sources & evidence

ORD record
ord-bb251e91b61745eaaa3691cfc801a4e2
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

Loading…