Chlorosulfamic acid → HCID 66746981, compound

HRID 1467255Notes

Reaction equation

HRID 1467255 reaction equation
[NH2:1][C:2]1[C:3]([C:19]#[N:20])=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][CH2:6][C:7]([NH:10][C:11]([NH:13][CH2:14][CH3:15])=[O:12])([CH3:9])[CH3:8].[S:21](Cl)(=[O:24])(=[O:23])[NH2:22]>>[S:21]([NH:1][C:2]1[C:3]([C:19]#[N:20])=[C:4]([CH:16]=[CH:17][CH:18]=1)[O:5][CH2:6][C:7]([NH:10][C:11]([NH:13][CH2:14][CH3:15])=[O:12])([CH3:8])[CH3:9])(=[O:24])(=[O:23])[NH2:22]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 66746425HCID 66746425, compound

Product 1

HCID 66746981HCID 66746981, compoundYield 100%

Procedure

Prepared as in Example 197a from 1-(1-(3-amino-2-cyanophenoxy)-2-methylpropan-2-yl)-3-ethylurea (Example 209b) and sulfamoyl chloride in 100% yield. MS 356 (MH+).

Sources & evidence

ORD record
ord-1d0cc80eb2aa4cf3a0c8b210d181cb74
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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