Dinitrobenzonitrile → HCID 66745912, compound

HRID 1467256Notes

Reaction equation

HRID 1467256 reaction equation
[CH2:1]([NH:3][C:4]([NH:6][C:7]([CH3:11])([CH3:10])[CH2:8][OH:9])=[O:5])[CH3:2].[N+:12]([C:15]1[CH:22]=[CH:21][CH:20]=[C:19]([N+]([O-])=O)[C:16]=1[C:17]#[N:18])([O-:14])=[O:13]>>[C:17]([C:16]1[C:15]([N+:12]([O-:14])=[O:13])=[CH:22][CH:21]=[CH:20][C:19]=1[O:9][CH2:8][C:7]([NH:6][C:4]([NH:3][CH2:1][CH3:2])=[O:5])([CH3:10])[CH3:11])#[N:18]

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 3661587HCID 3661587, compound

Product 1

HCID 66745912HCID 66745912, compoundYield 65%

Procedure

Prepared as in Example 197c from 1-ethyl-3-(1-hydroxy-2-methylpropan-2-yl)urea (Example 209d) and 2,6-dinitrobenzonitrile in 65% yield. MS 307 (MH+).

Sources & evidence

ORD record
ord-40b946103f994b3b830e77a1c7956c5d
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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