1,6-Hexanediol → HCID 66746992, compound

HRID 1467265Notes

Reaction equation

HRID 1467265 reaction equation
[CH2:1]([OH:8])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][OH:7].[N+:9]([C:12]1[CH:19]=[CH:18][CH:17]=[C:16]([N+]([O-])=O)[C:13]=1[C:14]#[N:15])([O-:11])=[O:10]>>[OH:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][O:8][C:16]1[CH:17]=[CH:18][CH:19]=[C:12]([N+:9]([O-:11])=[O:10])[C:13]=1[C:14]#[N:15]

Participants

3

Reactant 2

HCID 123741,6-HexanediolHCID 520718Dinitrobenzonitrile

Product 1

HCID 66746992HCID 66746992, compoundYield 88%

Procedure

Prepared as in Example 197c from hexane-1,6-diol and 2,6-dinitrobenzonitrile in 88% yield as a pale yellow solid. MS 265 (MH+).

Sources & evidence

ORD record
ord-e215d8af2da04b48be1d5634e323cc39
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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