1-Propanol, 3-amino-2,2-dimethyl- → 1-(3-Hydroxy-2,2-dimethylpropyl)-3-(4-methoxybenzyl)urea

HRID 1467271Notes

Reaction equation

HRID 1467271 reaction equation
[NH2:1][CH2:2][C:3]([CH3:7])([CH3:6])[CH2:4][OH:5].[CH3:8][O:9][C:10]1[CH:19]=[CH:18][C:13]([CH2:14][N:15]=[C:16]=[O:17])=[CH:12][CH:11]=1>>[OH:5][CH2:4][C:3]([CH3:7])([CH3:6])[CH2:2][NH:1][C:16]([NH:15][CH2:14][C:13]1[CH:18]=[CH:19][C:10]([O:9][CH3:8])=[CH:11][CH:12]=1)=[O:17]

Participants

3

Reactant 2

HCID 1173261-Propanol, 3-amino-2,2-dimethyl-HCID 187910Isocyanic acid, p-methoxybenzyl-

Product 1

HCID 667472421-(3-Hydroxy-2,2-dimethylpropyl)-3-(4-methoxybenzyl)ureaYield 100%

Procedure

Prepared as in Example 206d from 3-amino-2,2-dimethylpropan-1-ol and 4-methoxybenzyl isocyanate in 100% yield. MS 267 (MH+).

Sources & evidence

ORD record
ord-a739cd1c4c004e1d8304823d6d335438
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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