2-(3,5-Dimethyl-1H-pyrazol-1-yl)ethan-1-ol → HCID 66746772, compound

HRID 1467291Notes

Reaction equation

HRID 1467291 reaction equation
[CH3:1][C:2]1[CH:6]=[C:5]([CH3:7])[N:4]([CH2:8][CH2:9][OH:10])[N:3]=1.[N+:11]([C:14]1[CH:21]=[CH:20][CH:19]=[C:18]([N+]([O-])=O)[C:15]=1[C:16]#[N:17])([O-:13])=[O:12]>>[CH3:1][C:2]1[CH:6]=[C:5]([CH3:7])[N:4]([CH2:8][CH2:9][O:10][C:18]2[CH:19]=[CH:20][CH:21]=[C:14]([N+:11]([O-:13])=[O:12])[C:15]=2[C:16]#[N:17])[N:3]=1

Participants

3

Reactant 2

HCID 2596652-(3,5-Dimethyl-1H-pyrazol-1-yl)ethan-1-olHCID 520718Dinitrobenzonitrile

Product 1

HCID 66746772HCID 66746772, compoundYield 90.7%

Procedure

Prepared as in Example 197c from 2-(3,5-dimethyl-1H-pyrazol-1-yl)ethanol and 2,6-dinitrobenzonitrile in 90.7% yield. MS 287 (MH+).

Sources & evidence

ORD record
ord-7f2bc3ca23fa4f198e1c45cbe4d32555
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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