Chlorosulfamic acid → HCID 66745893, compound

HRID 1467294Notes

Reaction equation

HRID 1467294 reaction equation
[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([O:10][CH2:11][CH2:12][CH2:13][S:14][CH3:15])[C:3]=1[C:4]#[N:5].[S:16](Cl)(=[O:19])(=[O:18])[NH2:17]>>[S:16]([NH:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([O:10][CH2:11][CH2:12][CH2:13][S:14][CH3:15])[C:3]=1[C:4]#[N:5])(=[O:19])(=[O:18])[NH2:17]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 66746883HCID 66746883, compound

Product 1

HCID 66745893HCID 66745893, compoundYield 69%

Procedure

Prepared as in Example 197a from 2-amino-6-(3-(methylthio)propoxy)benzonitrile (Example 234b) and sulfamoyl chloride in 69% yield. MS 302 (MH+).

Sources & evidence

ORD record
ord-4e8b42d7bfb54bd7868e49e1f26c9fac
Source dataset
uspto-grants-2015_04
Patent number
US09000054B2

Reaction notes

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