HCID 51035652, compound → HCID 178482744, compound

HRID 1467950Notes

Reaction equation

HRID 1467950 reaction equation
C(=O)([O:7][C:8]1[N:12]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=2)[N:11]=[C:10]([C:19]2[CH:20]=[C:21]([C:25]3[CH:30]=[CH:29][CH:28]=[C:27]([N:31]([CH3:33])[CH3:32])[CH:26]=3)[CH:22]=[CH:23][CH:24]=2)[CH:9]=1)OC(C)(C)C.C(=O)(OC(C)(C)C)OC1N(C2C=CC=CN=2)N=C(C2C=CC(C3C=CC=CC=3)=CC=2)C=1>>[CH3:32][N:31]([CH3:33])[C:27]1[CH:26]=[C:25]([C:21]2[CH:22]=[CH:23][CH:24]=[C:19]([C:10]3[CH:9]=[C:8]([OH:7])[N:12]([C:13]4[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=4)[N:11]=3)[CH:20]=2)[CH:30]=[CH:29][CH:28]=1

Participants

3

Reactant 2

HCID 51035652HCID 51035652, compoundHCID 51038617HCID 51038617, compound

Product 1

HCID 178482744HCID 178482744, compoundYield 99%

Procedure

The title compound was prepared in the same manner as in Example D-1, except that an equimolar amount of Compound 42 of Example C-16 was used in place of Compound 27 of Example C-1.

Sources & evidence

ORD record
ord-8af78ee045064ddf9fe7a9ed3624e112
Source dataset
uspto-grants-2015_04
Patent number
US09000176B2

Reaction notes

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