HCID 51035654, compound → HCID 178515523, compound

HRID 1467952Notes

Reaction equation

HRID 1467952 reaction equation
C(=O)(OC(C)(C)C)[O:2][C:3]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=2)[N:6]=[C:5]([C:14]2[CH:19]=[CH:18][C:17]([C:20]3[CH:25]=[CH:24][C:23]([O:26][CH2:27][C:28]4[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=4)=[CH:22][CH:21]=3)=[CH:16][CH:15]=2)[CH:4]=1.C(=O)(OC(C)(C)C)OC1N(C2C=CC=CN=2)N=C(C2C=CC(C3C=CC=CC=3)=CC=2)C=1>>[CH2:27]([O:26][C:23]1[CH:22]=[CH:21][C:20]([C:17]2[CH:18]=[CH:19][C:14]([C:5]3[CH:4]=[C:3]([OH:2])[N:7]([C:8]4[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=4)[N:6]=3)=[CH:15][CH:16]=2)=[CH:25][CH:24]=1)[C:28]1[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=1

Participants

3

Reactant 2

HCID 51035654HCID 51035654, compoundHCID 51038617HCID 51038617, compound

Product 1

HCID 178515523HCID 178515523, compoundYield 85%

Procedure

The title compound was prepared in the same manner as in Example D-1, except that an equimolar amount of Compound 44 of Example C-18 was used in place of Compound 27 of Example C-1.

Sources & evidence

ORD record
ord-3ce69543c2e3474fbc6ad1f35b5492fb
Source dataset
uspto-grants-2015_04
Patent number
US09000176B2

Reaction notes

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