HCID 51038617, compound → HCID 178515518, compound

HRID 1467957Notes

Reaction equation

HRID 1467957 reaction equation
C(=O)(OC(C)(C)C)[O:2][C:3]1[N:7]([C:8]2[N:13]=[CH:12][CH:11]=[CH:10][N:9]=2)[N:6]=[C:5]([C:14]2[CH:19]=[CH:18][C:17]([C:20]3[CH:25]=[CH:24][CH:23]=[C:22]([C:26]4[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=4)[CH:21]=3)=[CH:16][CH:15]=2)[CH:4]=1.C(=O)(OC(C)(C)C)OC1N(C2C=CC=CN=2)N=C(C2C=CC(C3C=CC=CC=3)=CC=2)C=1>>[C:26]1([C:22]2[CH:21]=[C:20]([C:17]3[CH:16]=[CH:15][C:14]([C:5]4[CH:4]=[C:3]([OH:2])[N:7]([C:8]5[N:9]=[CH:10][CH:11]=[CH:12][N:13]=5)[N:6]=4)=[CH:19][CH:18]=3)[CH:25]=[CH:24][CH:23]=2)[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=1

Participants

3

Reactant 2

HCID 51038617HCID 51038617, compoundHCID 68193707HCID 68193707, compound

Product 1

HCID 178515518HCID 178515518, compoundYield 93%

Procedure

The title compound was prepared in the same manner as in Example D-1, except that an equimolar amount of Compound 50 of Example C-24 was used in place of Compound 27 of Example C-1.

Sources & evidence

ORD record
ord-d9d0a200344645d381cd2ef325e411a0
Source dataset
uspto-grants-2015_04
Patent number
US09000176B2

Reaction notes

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